114 parts per million in or on apples, apricots, asparagus, beans, beets (with or without tops) or beet greens alone, blackberries, blueberries (huckleberries), boysenberries, broccoli, brussels sprouts, cabbage, carrots, cauliflower, cherries, collards, corn, cranberries, cucumbers, currants, dewberries, eggplants, gooseberries, grapes, kale, kohlrabi, lettuce, loganberries, melons, mushrooms, nectarines, peaches, peanuts, pears, peas, peppers, pineapples, plums (fresh prunes), pumpkins, quinces, radishes (with or without tops) or radish tops, raspberries, rutabagas (with or without tops) or rutabaga tops, spinach, squash, strawberries, summer squash, tomatoes, turnips (with or without tops) or turnip greens, youngberries.

7 parts per million in or on sweetpotatoes and yams from preharvest and postharvest application.

3 parts per million in or on the fat of meat from cattle, goats, hogs, horses, or sheep.

2 parts per million in or on the following grains from storage-bin treatment: Barley, corn, oats, rice, rye, sorghum grain, wheat.

1 part per million in or on potatoes. Zero in milk.

§ 180.121

Parathion or its methyl homolog; tolerances for residues.

Tolerances for residues of the insecticide parathion (0,0-diethyl-O-p-nitrophenyl thiophosphate) or its methyl homolog in or on raw agricultural commodities are established as follows:

5 parts per million in or on alfalfa hay. 1.25 parts per million in or on alfalfa (fresh).

1 part per million in or on apples, apricots, artichokes, avocados, barley, beans, beets (with or without tops) or beet greens alone, blackberries, blueberries (huckleberries), boysenberries, broccoli, brussels sprouts, cabbage, carrots, cauliflower, celery, cherries, citrus fruits, clover, collards, corn, corn forage, cranberries, cucumbers, currants, dates, dewberries, eggplants, endive (escarole), figs, garlic, gooseberries, grapes, grass for forage, guavas, hops, kale, kohlrabi, lettuce, loganberries, mangoes, rnelons, mustard greens, nectarines, oats, okra, olives, onions, parsnips (with or without tops) or parsnip greens alone, peaches, pea forage, peanuts, pears, peas, peppers, pineapples, plums, (fresh prunes),

1 See footnote 1 to § 180.115.

pumpkins, quinces, radishes (with or without tops) or radish tops, raspberries, rice, rutabagas (with or without tops) or rutabaga tops, soybean hay, spinach, squash, strawberries, summer squash, Swiss chard, tomatoes, turnips (with or without tops) or turnip greens, vetch, wheat, youngberries.

0.75 part per million in or on cottonseed.

0.2 part per million in or on sunflower seed.

0.1 part per million in or on soybeans. [36 FR 22540, Nov. 25, 1971, as amended at 37 FR 5496, Mar. 16, 1972]

A tolerance of 0.3 part per million is established for residues of the insecticide chlordane (1,2,4,5,6,7,8,8-octachloro-2,3,

3a,4,7,7a-hexahydro-4,7-methanoindene, containing not more than 1 percent of the intermediate compound hexachlorocyclopentadiene) in or on each of the following raw agricultural commodities: Apples, apricots, beans, beets (with or without tops) or beet greens alone, blackberries, blueberries (huckleberries), boysenberries, broccoli, brussels sprouts, cabbage, carrots, cauliflower, celery, cherries, citrus fruits, collards, corn, cucumbers, dewberries, eggplants, grapes, kale, kohlrabi, lettuce, loganberries, melons, nectarines, okra, onions, papayas, peaches, peanuts, pears, peas, peppers, pineapples, plums (fresh prunes), potatoes, quinces, radishes (with or without tops) or radish tops, raspberries, rutabagas (with or without tops) or rutabaga tops, squash, strawberries, summer squash, sweetpotatoes, tomatoes, turnips (with or without tops) or turnip greens, youngberries.

§ 180.123 Inorganic bromides resulting from fumigation with methyl bromide; tolerances for residues. Tolerances for residues of inorganic bromides (calculated as Br) in or on raw agricultural commodities that have been fumigated with the antimicrobial agent and insecticide methyl bromide after harvest (with the exception of strawberries) are established as follows: 240 parts per million in or popcorn.

on

100 parts per million in or on asparagus, cumin seed, and ginger root from use in accordance with the Plant Quarantine Program of the U.S. Department of Agriculture.

75 parts per million in or on potatoes, sweetpotatoes.

75 parts per million in or on avacados and coffee beans from use in accordance with the Plant Quarantine Program of the U.S. Department of Agriculture.

50 parts per million in or on alfalfa hay, barley, beans, beans (green), beans (lima), beans (snap), black-eyed peas, cipollini bulbs, cocoa beans, corn, garlic, grain sorghum (milo), oats, peas, rice, rye, sweet corn (determined on kernels plus cob with husk removed), wheat.

50 parts per million in or on cabbage from use in accordance with the Plant Quarantine Program of the U.S. Department of Agriculture.

50 parts per million in or on timothy hay from use in accordance with the Plant Pest Control Program of the U.S. Department of Agriculture.

30 parts per million in or on garden beets (roots), carrots, citrus citron, cucumbers, grapefruit, horseradish, Jerusalem-artichokes, kumquats, lemons, limes, okra, oranges, parsnips (roots), peppers, pimentos, radishes, rutabagas, salsify roots, strawberries (from use before harvest), sugar beets (roots), summer squash, tangerines, turnips (roots), yams.

20 parts per million in or on apricots, cantaloups, cherries, eggplants, grapes, honeydew melons, mangoes, muskmelons, nectarines, onions, papayas, peaches, pineapples, plums (fresh prunes), pumpkins, tomatoes, watermelons, winter squash, zucchini squash.

5 parts per million in or on apples, pears, quinces.

[36 FR 22540, Nov. 25, 1971, as amended at 37 FR 24183, Nov. 15, 1972]

§ 180.124 Glyodin; tolerances for residues.

Tolerances are established for residues of the fungicide glyodin (2-heptadecyl glyoxalidine acetate or 2-heptadecyl glyoxalidine (base)) in or on the raw agricultural commodities apples, cher

ries, peaches, and pears at 5 parts per million.

§ 180.125 Calcium cyanide; tolerances for residues.

Tolerances are established for residues of the insecticide calcium cyanide, calculated as hydrogen cyanide, in or on raw agricultural commodities as follows:

25 parts per million, from postharvest application, in or on the grains: Barley, buckwheat, corn, oats, rice, rye, sorghum, and wheat.

5 parts per million in or on cucumbers, lettuce, radishes, and tomatoes. § 180.126 Inorganic bromides resulting from soil treatment with ethylene dibromide; tolerances for residues. Tolerances for residues of inorganic bromides (calculated as Br) in or on raw agricultural commodities grown in soil treated with the nematocide ethylene dibromide are established as follows:

75 parts per million in or on broccoli, carrots, melons, parsnips, potatoes.

50 parts per million in or on eggplant, okra, summer squash, sweet corn, sweet corn forage, sweetpotatoes, tomatoes.

40 parts per million in or on pineapple. 30 parts per million in or on cucumbers, lettuce, peppers.

25 parts per million in or on cottonseed, peanuts (see § 180.126a).

10 parts per million in or on asparagus, cauliflower.

5 parts per million in or on lima beans, strawberries.

§ 180.126a Inorganic bromide residues in peanut hay and peanut hulls; statement of policy.

(a) Investigations by the Food and Drug Administration show that peanut hay and peanut hulls have been used as feed for meat and dairy animals. While many growers now harvest peanuts with combines and leave the hay on the ground to be incorporated into the soil, some growers follow the practice of curing peanuts on the vines in a stack and save the hay for animal feed. Peanut shells or hulls have been used to a minor extent as roughage for cattle feed. It has been established that the feeding to cattle of peanut hay and peanut hulls containing residues of inorganic bromides will contribute considerable residues of inorganic bromides to the meat and milk.

(b) There are no tolerances for inorganic bromides in meat and milk to

cover residues from use of such peanut hay and peanut hulls as animal feed. Peanut hay and peanut hulls containing residues of inorganic bromides from the use of nematocides such as ethylene dibromide or 1,2-dibromo-3-chloropropane are unsuitable as an ingredient in the feed of meat and dairy animals and should not be represented, sold, or used for that purpose.

§ 180.127 Piperonyl butoxide; tolerances for residues.

Tolerances for residues of the insecticide piperonyl butoxide ((butyl carbityl) (6-propyl piperonyl) ether) are established in or on raw agricultural commodities, as follows:

20 parts per million from postharvest application in or on barley, birdseed mixtures, buckwheat, corn (including popcorn), rice, rye, wheat.

8 parts per million from postharvest application in or on almonds, apples, beans, blackberries, blueberries (huckleberries), boysenberries, cherries, cocoa beans, copra, cottenseed, crabapples, currants, dewberries, figs, flaxseed, gooseberries, gran sorghum, grapes, guavas, loganberries, mangoes, muskmelons, oats, oranges, peaches, peanuts (determined on the nuts with shell removed), pears, peas, pineapples, plums (fresh prunes), raspberries, tomatoes, walnuts. 3 parts per million in meat, fat, and meat byproducts of poultry.

1 part per million in eggs. 0.25 part per million from postharvest application in or on potatoes.

0.25 part per million (reflecting negligible residues in milk) in milk fat.

0.1 part per million (negligible residue) in the meat, fat, and meat byproducts of cattle, goats, hogs, horses, and sheep. [37 FR 738, Jan. 18, 1972, as amended at 37 FR 11724, June 13, 1972]

§ 180.128 Pyrethrins; tolerances for

Tolerances for residues of the insecticide pyrethrins (insecticidally active principles of Chrysanthemum cinerariaefolium) are established in or on raw agricultural commodities as follows:

From postharvest application: 3 parts per million in or on barley, birdseed mixtures, buckwheat, corn (including popcorn), rice, rye, and wheat.

From postharvest application: 1 part per million in or on almonds, apples, beans, blackberries, blueberries (huckleberries), boysenberries, cherries, cocoa beans, copra, cottonseed, crabapples,

currants, dewberries, figs, flaxseed, gooseberries, grain sorghum, grapes, guavas, loganberries, mangoes, muskmelons, oats, oranges, peaches, peanuts (determined on the nuts with shell removed), pears, peas, pineapples, plums (fresh prunes), raspberries, tomatoes, and walnuts.

0.5 part per million in milk fat reflecting negligible residues in milk.

0.2 part per million in meat, fat, and meat byproducts of poultry.

0.1 part per million (negligible residue) in eggs and meat, fat and meat byproducts of cattle, goats, hogs, horses, and sheep.

0.05 part per million in or on potatoes from postharvest application.

[36 FR 22540, Nov. 25, 1971, as amended at 37 FR 11724, June 13, 1972]

§ 180.129 o-Phenylphenol and its sodium salt; tolerances for residues. Tolerances are established for residues of the fungicides o-phenylphenol and sodium o-phenylphenate, each expressed as o-phenylphenol, from postharvest application of either, as follows:

125 parts per million in or on cantaloups, of which not more than 10 parts per million shall be in the edible portion. 25 parts per million in or on apples, pears.

20 parts per million in or on carrots, peaches, plums (fresh prunes).

15 parts per million in or on sweetpotatoes.

10 parts per million in or on citrus citron, cucumbers, grapefruit, kumquats, lemons, limes, oranges, peppers (bell), pineapples, tangerines, tomatoes.

5 parts per million in or on cherries, nectarines.

§ 180.130 Hydrogen cyanide; tolerances for residues.

Tolerances for residues of the insecticide hydrogen cyanide from postharvest fumigation are established as follows:

250 parts per million in or on the following spices: Allspice, anise, basil, bay, black pepper, caraway, cassia, celery seed, chili, cinnamon, cloves, coriander, cumin, dill, ginger, mace, marjoram, nutmeg, oregano, paprika, poppy, red pepper, rosemary, sage, savory, thyme, tumeric, white pepper.

75 parts per million in or on barley, buckwheat, corn (including popcorn), milo (grain sorghum), oats, rice, rye, wheat.

50 parts per million in or on citrus fruits.

25 parts per million in or on almonds, beans (dried), cashews, cocoa beans, peanuts, peas (dried), pecans, sesame, walnuts.

§ 180.131 Endrin; tolerances for residues.

A tolerance of zero is established for residues of the insecticide endrin in or on each of the following raw agricultural commodities: Broccoli, brussels sprouts, cabbage, cauliflower, cottonseed, cucumbers, eggplant, peppers, potatoes, sugarbeets, sugarbeet tops, summer squash, and tomatoes.

§ 180.132 Thiram; tolerances for residues.

Tolerances for residues of the fungicide thiram (tetramethyl thiuram disulfide) in or on raw agricultural commodities are established as follows:

7 parts per million in or on apples, celery, peaches, strawberries, tomatoes.

7 parts per million in or on bananas, (from preharvest and postharvest application) of which not more than 1 part per million shall be in the pulp after peel is removed and discarded.

0.5 part per million in or on onions (dry bulb).

[36 FR 22540, Nov. 25, 1972, as amended at 37 FR 3182, Feb. 12, 1972]

Tolerances are established for residues of the insecticide lindane (gamma isomer of benzene hexachloride) in or on raw agricultural commodities as follows:

7 parts per million in or on the fat of meat from cattle, goats, horses, and sheep.

4 parts per million in or on the fat of meat from hogs.

3 parts per million in or on cucumbers, lettuce, melons, mushrooms, pumpkins, squash, summer squash, and tomatoes.

1 part per million in or on apples, apricots, asparagus, avocados, broccoli, brussels sprouts, cabbage, cauliflower, celery, cherries, collards, eggplants, grapes, guavas, kale, kohlrabi, mangoes, mustard greens, nectarines, okra, onions (dry bulb only), peaches, pears, peppers, pineapples, plums (fresh prunes), quinces, spinach, strawberries, and Swiss chard.

§ 180.134 Ovex; tolerances for residues.

Tolerances for residues of the insecticide ovex (p-chlorophenyl-p-chlorobenzenesulfonate) are established as fol

lows:

5 parts per million in or on grapefruit, lemons, oranges, tangerines

3 parts per million in or on apples, peaches, pears, plums (fresh prunes). § 180.135 Aldrin; tolerances for residues.

Tolerances for total residues of the insecticide aldrin and its epoxidation product dieldrin, resulting from application of aldrin, in or on raw agricultural commodities are established as follows:

0.1 part per million in or on asparagus, broccoli, brussels sprouts, cabbage, cantaloups, cauliflower, celery, cherries, cranberries, cucumbers, eggplant, grapes, lettuce, mangoes, muskmelons, nectarines, peaches, peppers, pimentos, pineapple, plums (fresh prunes), potatoes, pumpkins, strawberries, summer squash, sweet potatoes, tomatoes, watermelons, winter squash.

Zero in or on alfalfa, apples, apricots, beans, black-eyed peas, carrots, clover, collards, corn forage, corn grain, cowpeas, cowpea hay, endive (escarole), garden beets, garden beet tops, garlic, grain sorghum, grain sorghum forage, horse radish, kale, kohlrabi, leeks, lespedeza, mustard greens, onions, parsnips, peanuts, peanut hay, pears, peas, pea hay, popcorn, quinces, radishes, rutabagas, salsify tops, salsify roots, shallots, soybeans, soybean hay, spinach, sugarbeets, sugarbeet tops, Swiss chard,

turnips, turnip tops.

Additional tolerances for total residues of aldrin are established, on an interim basis pending reevaluation of all tolerances for this insecticide when new toxicity and related data become available on or before June 30, 1968, at 0.1 part per million in or on straws of barley, oats, rice, rye, and wheat; at 0.05 part per million in or on grapefruit, lemons, limes, oranges, rice grain, and tangerines; at 0.02 part per million in or on the grains of barley, oats, rye, and wheat. § 130.136 Basic copper carbonate; tolerance for residues.

The tolerance for residues of the fungicide basic copper carbonate in or on pears from post-harvest use of the chemical is 3 parts per million of combined copper.

§ 180.137 Dieldrin; tolerances for residues.

Tolerances for residues of the insecticide dieldrin in or on raw agricultural commodities are established as follows:

0.1 part per million in or on apples, apricots, asparagus, bananas, broccoli, brussels sprouts, cabbage, carrots, cauliflower, cherries, cranberries, cucumbers, eggplant, grapes, horse radish, lettuce, mangoes, nectarines, onions, parsnips, peaches, pears, peppers, pimentos, plums (fresh prunes), potatoes, quinces, radishes, radish tops, salsify roots, strawberries, summer squash, sweet potatoes, tomatoes.

Zero in or on alfalfa, beans, black-eyed peas, clover, collards, corn grain, corn forage, cowpeas, cowpea hay, endive (escarole), garden beets, garden beet tops, grain sorghum, grain sorghum forage, kale, kohlrabi, lespedeza, mustard greens, peas, pea hay, popcorn, rutabagas, salsify tops, spinach, soybeans, soybean hay, Swiss chard, turnips, turnip tops.

Additional tolerances for residue of dieldrin are established, on an interim basis pending reevaluation of all tolerances for this insecticide when new toxicity and related data become available on or before June 30, 1968, at 0.1 part per million in or on the straws of barley, oats, rye, and wheat; at 0.05 part per million in or on grapefruit, lemons, limes, oranges, and tangerines; at 0.02 part per million in or on the grains of barley, oats, rye, and wheat.

§ 180.138 Toxaphene; tolerances for residues.

Tolerances are established for residues of the insecticide toxaphene (chlorinated camphene containing 67 percent-69 percent chlorine) in or on raw agricultural commodities as follows:

17 parts per million in or on apples, apricots, beans, blackberries, boysenberries, broccoli, brussels sprouts, cabbage, carrots, cauliflower, celery, citrus fruits, collards, corn, cranberries, cucumbers, dewberries, eggplants; fat of meat from cattle, goats, hogs, horses, and sheep; hazelnuts, hickory nuts, horseradish, kale, kohlrabi, lettuce, loganberries, nectarines, okra, onions, parsnips, peaches, peanuts, pears, peas, pecans, peppers, pimentos, quinces, radishes

1 See footnote 1 to § 180.115.

(with or without tops) or radish tops, raspberries, rutabagas, spinach, strawberries, tomatoes, walnuts, youngberries. 5 parts per million in or on barley, oats, rice, rye, sorghum grain, wheat.

5 parts per million, calculated as a chlorinated terpene of molecular weight 396.6 containing 67 percent chlorine, in or on cottonseed.

3.5 parts per million combined residues of DDT and toxaphene in or on soybeans (dry form), of which residues DDT shall not exceed 1.5 parts per million and toxsphene shall not exceed 2 parts per million.

3 parts per million in or on bananas (of which residue not more than 0.3 part per million shall be in the pulp after the peel is removed and discarded), pineapples.

2 parts per million in or on soybeans (dry form).

§ 180.139

1,1-Dichloro-2,2-bis(p-ethylphenyl) ethane; tolerances for residues.

Tolerances are established for residues of the insecticide 1,1-dichloro-2,2-bis (p-ethylphenyl) ethane in or on raw agricultural commodities as follows:

15 parts per million in or on apples, broccoli, brussels sprouts, cabbage, cauliflower, cherries, kohlrabi, lettuce, pears, spinach.

Zero in meat and milk.

§ 180.140 BHC; tolerances for residues.

Tolerances are established for residues of the insecticide BHC (benzene hexachloride) in or on the raw agricultural commodities apples, apricots, asparagus, avacodos, broccoli, brussels sprouts, cabbage, cauliflower, celery, cherries, collards, cucumbers, eggplants, grapes, kale, kohlrabi, lettuce, melons, mustard greens, nectarines, okra, onions (dry bulb only), peaches, pears, peppers, plums (fresh prunes), pumpkins, spinach, strawberries, squash, summer squash, Swiss chard, and tomatoes at 1 part per million.

§ 180.141 Biphenyl; tolerances for residues.

A tolerance of 110 parts per million for residues of the fungicide biphenyl (also known as diphenyl) from postharvest use is established in or on each of the following raw agricultural commodities: Citrus citron, grapefruit, kumquats, lemons, limes, oranges, tangerines, other citrus fruits and hybrids thereof.